Side-chain reporters worth knowing

Asp / Glu carboxyls switch between ~1716/1712 (protonated C=O) and ~1574/1560 + ~1402/1404 (ionised COO⁻) — direct pKa / H-bond probes. Arg guanidinium 1673/1633 and Lys ammonium 1629/1526 mark charged residues. Tyr 1518/1250 reports ring protonation; Asn/Gln add side-chain amide carbonyls that overlap amide I.

CodeAmino acidClassDiagnostic bands (cm⁻¹)NoteMeasured ↗

Measured amino-acid IR

Amino acids are involatile, so they are absent from the gas-phase NIST experimental database — these entries are reconstructions from literature positions. Real solid-state / aqueous FTIR for each residue is reachable via the Measured ↗ links above (SDBS, SpectraBase).

Simulate & compare

Tick residues to overlay their reconstructed spectra. Defaults compare an acidic (Asp), a basic (Arg) and an aromatic (Tyr) side chain.

Backbone amide modes for assembled chains are on the protein IR page; the full simulator with bases and backbones is at simulate.

References

  1. Barth, A. The infrared absorption of amino acid side chains, Prog. Biophys. Mol. Biol. 74 (2000) 141.
  2. Barth, A. Infrared spectroscopy of proteins, Biochim. Biophys. Acta 1767 (2007) 1073.
  3. Venyaminov, S. & Kalnin, N. Quantitative IR spectrophotometry of peptide compounds, Biopolymers 30 (1990) 1243.